DIN EN 15652-2009 食品.高效液相色谱法(HPLC)测定烟酸.英文版本DINEN15652-2009-09
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【英文标准名称】:Foodstuffs-DeterminationofniacinbyHPLC;EnglishversionofDINEN15652:2009-09
【原文标准名称】:食品.高效液相色谱法(HPLC)测定烟酸.英文版本DINEN15652-2009-09
【标准号】:DINEN15652-2009
【标准状态】:现行
【国别】:德国
【发布日期】:2009-09
【实施或试行日期】:
【发布单位】:德国标准化学会(DE-DIN)
【起草单位】:
【标准类型】:()
【标准水平】:()
【中文主题词】:化学分析和试验;比较;比较分析法;测定;含量测定;萃取;食品检验;食品;高效液相色谱法;高效液相色谱分析法(HPLC);水解;质量浓度;数学计算;分析方法;烟酰胺;精密度;复合维生素B;维生素
【英文主题词】:Chemicalanalysisandtesting;Comparison;Comparisonanalysis;Determination;Determinationofcontent;Extraction;Foodinspection;Foodproducts;Highperformanceliquidchromatography;HPLC;Hydrolysis;Massconcentration;Mathematicalcalculations;Methodsofanalysis;Nicotinamide;Precision;VitaminBcomplex;Vitamins
【摘要】:ThisEuropeanStandardspecifiesamethodforthedeterminationofthemassfractionofniacininfoodstuffsbyhighperformanceliquidchromatography(HPLC)bythreedifferentwaysofhydrolysis,acidhydrolysis(A),enzymatichydrolysis(B)oracid/alkalinehydrolysis(C).Themethodhasbeenvalidatedininterlaboratorytestsonfortifiedandnon-fortifiedsamplessuchasbreakfastcerealpowder,chocolatecereals,cookedham,greenpeas,lyophilizedgreenpeaswithham,lyophilizedsoup,nutritiveorangejuice,milkpowderandwheatflour,atlevelsfrom0,5mg/1O0gto24mg/100g.Forfurtherinformationonthevalidationdata,seeAnnexB.AandBgivesimilarresultsforniacin.InoptionsAandBniaciniscalculatedasthesumofnicotinamideandnicotinicacid,andexpressedasnicotinicacid[1].OptionCgiveshigherresultsthanAandBforniacinwithnon-supplementedcereals,butsimilarresultsforotherproducts,InoptionC,niaciniscalculatedandexpressedasnicotinicacidaftertransformationofnicotinamideintonicotinicacid[2].OptionAisfasterandcheaperthanBandC.OptionBisusedifanexactquantificationofnicotinamideandnicotinicacidisneeded.ThiscannotbedonewithoptionA,becausethereisaslighttransformationofnicotinamideintonicotinicacidduringtheacidhydrolysis.OptionCquantifiestotalniacin.Thealkalinehydrolysisisabletoliberateotherformsgivinghigherresultsforniacin,whichinsomefoodssuchasmaizeandcerealsarenotnormallybiologicallyavailable,see[3],[4]and[5].InformationonacomparisonbetweenthethreedifferentwaysofhydrolysisisgiveninAnnexC.
【中国标准分类号】:X04
【国际标准分类号】:67_050
【页数】:23P.;A4
【正文语种】:英语
【原文标准名称】:食品.高效液相色谱法(HPLC)测定烟酸.英文版本DINEN15652-2009-09
【标准号】:DINEN15652-2009
【标准状态】:现行
【国别】:德国
【发布日期】:2009-09
【实施或试行日期】:
【发布单位】:德国标准化学会(DE-DIN)
【起草单位】:
【标准类型】:()
【标准水平】:()
【中文主题词】:化学分析和试验;比较;比较分析法;测定;含量测定;萃取;食品检验;食品;高效液相色谱法;高效液相色谱分析法(HPLC);水解;质量浓度;数学计算;分析方法;烟酰胺;精密度;复合维生素B;维生素
【英文主题词】:Chemicalanalysisandtesting;Comparison;Comparisonanalysis;Determination;Determinationofcontent;Extraction;Foodinspection;Foodproducts;Highperformanceliquidchromatography;HPLC;Hydrolysis;Massconcentration;Mathematicalcalculations;Methodsofanalysis;Nicotinamide;Precision;VitaminBcomplex;Vitamins
【摘要】:ThisEuropeanStandardspecifiesamethodforthedeterminationofthemassfractionofniacininfoodstuffsbyhighperformanceliquidchromatography(HPLC)bythreedifferentwaysofhydrolysis,acidhydrolysis(A),enzymatichydrolysis(B)oracid/alkalinehydrolysis(C).Themethodhasbeenvalidatedininterlaboratorytestsonfortifiedandnon-fortifiedsamplessuchasbreakfastcerealpowder,chocolatecereals,cookedham,greenpeas,lyophilizedgreenpeaswithham,lyophilizedsoup,nutritiveorangejuice,milkpowderandwheatflour,atlevelsfrom0,5mg/1O0gto24mg/100g.Forfurtherinformationonthevalidationdata,seeAnnexB.AandBgivesimilarresultsforniacin.InoptionsAandBniaciniscalculatedasthesumofnicotinamideandnicotinicacid,andexpressedasnicotinicacid[1].OptionCgiveshigherresultsthanAandBforniacinwithnon-supplementedcereals,butsimilarresultsforotherproducts,InoptionC,niaciniscalculatedandexpressedasnicotinicacidaftertransformationofnicotinamideintonicotinicacid[2].OptionAisfasterandcheaperthanBandC.OptionBisusedifanexactquantificationofnicotinamideandnicotinicacidisneeded.ThiscannotbedonewithoptionA,becausethereisaslighttransformationofnicotinamideintonicotinicacidduringtheacidhydrolysis.OptionCquantifiestotalniacin.Thealkalinehydrolysisisabletoliberateotherformsgivinghigherresultsforniacin,whichinsomefoodssuchasmaizeandcerealsarenotnormallybiologicallyavailable,see[3],[4]and[5].InformationonacomparisonbetweenthethreedifferentwaysofhydrolysisisgiveninAnnexC.
【中国标准分类号】:X04
【国际标准分类号】:67_050
【页数】:23P.;A4
【正文语种】:英语
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